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</o:shapelayout></xml><![endif]--></head><body lang=EN-CA link=blue vlink=purple><div class=WordSection1><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>Dear Jed and All<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>First, indirect greetings to Alexis – he will be a big asset for you.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>Looking over the interchange with Kevin this morning I am reminded of a setup I saw once that was distilling ethanol so I am adding this suggestion that is worth experimenting with. Might not work but you never know, so…<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>When you have the pipe coming out of the centre, you can run it vertically and if possible a bit larger than the normal ‘still’ pipe. The idea is to get the water to condense and fall back into the ‘mash’. If you have a bubbling pot with the lowest heat needed to keep it in that condition, it is inevitable that you will get a lot of water droplets and vapour in the gas mix.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>The idea is to keep the bubbling pot going while reducing the amount of water that is expelled into the condenser. So, the plan is to cool the rising gas in a vertical column before it is liquefied in the condenser. The use of a vertical metal pipe, possibly cooled a bit, but not much, will achieve the higher ethanol and lower water content you are seeking.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>If you have a thermometer at the top of the pipe, run the fire so the temperature at the top is a little below the local boiling point of water. This will help the water vapour condense and drop back into the mash without taking much of the ethanol vapour with it. It is basically a very simple form of fractional distillation.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>There is no reason it cannot be done horizontally however there is more natural cooling available on a vertical pipe than a nearly horizontal pipe of the same length.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>Under ideal conditions you can get 95% ethanol with this method. As long as there is some cooling and the exit temperature is below water boiling, and above ethanol boiling, you will get the fraction you want.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>I understand from the guys at the Simunye Sugar Estate in Swaziland that there are a large number of other ‘alcohols’ which are present in the ethanol – more than a dozen of them – but I am not sure if you will ever be able to separate them, or get the ‘cut’ you want except by watching the exit temperature at the top of the vertical/slanted tube.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>It may be that eventually after experimenting you will have a 2 metre copper pipe travelling upwards from the top of the pot before it turns down to the condenser. This trick is probably how distillers got a high ethanol content in a single pass.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>Doing a second pass with the ethanol alone can give 99% with similar control on the exit temperature. The guys doing this told me the highest they can get in one pass is 95% and that is why (because of energy cost) ethanol sold for stoves is never higher than that – it is made by the ‘cheap method’.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>We are of course interested to hear how this goes! It is certainly an unusual application.<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'>Regards<br>Crispin<o:p></o:p></span></p><p class=MsoNormal><span style='font-size:11.0pt;font-family:"Calibri","sans-serif";color:#1F497D'><o:p> </o:p></span></p></div></body></html>